Szczegóły publikacji

Opis bibliograficzny

Structural transformation of synthetic hydroxyapatite under simulated in vivo conditions studied with ATR-FTIR spectroscopic imaging / Anna Sroka-Bartnicka, Leszek Borkowski, Grażyna Ginalska, Anna ŚLÓSARCZYK, Sergei G. Kazarian // Spectrochimica Acta. Part A, Molecular and Biomolecular Spectroscopy ; ISSN 1386-1425. — 2017 — vol. 171, s. 155–161. — Bibliogr. s. 160–161, Abstr. — Publikacja dostępna online od: 2016-08-02

Autorzy (5)

Słowa kluczowe

infrared spectroscopystructural transformationhydroxyapatitebiomaterialscompositesATR-FTIR imaging

Dane bibliometryczne

ID BaDAP104833
Data dodania do BaDAP2017-04-25
Tekst źródłowyURL
DOI10.1016/j.saa.2016.07.051
Rok publikacji2017
Typ publikacjiartykuł w czasopiśmie
Otwarty dostęptak
Czasopismo/seriaSpectrochimica Acta, Part A, Molecular and Biomolecular Spectroscopy

Abstract

Hydroxyapatite and carbonate-substituted hydroxyapatite are widely used in bone tissue engineering and regenerative medicine. Both apatite materials were embedded into recently developed ceramic/polymer composites, subjected to Simulated Body Fluid (SBF) for 30 days and characterized using ATR-FTIR spectroscopic imaging to assess their behaviour and structures. The specific aim was to detect the transition phases between both types of hydroxyapatite during the test and to analyze the surface modification caused by SBF. ATR-FTIR spectroscopic imaging was successfully applied to characterise changes in the hydroxyapatite lattice due to the elastic properties of the scaffolds. It was observed that SBF treatment caused a replacement of phosphates in the lattice of non-substituted hydroxyapatite by carbonate ions. A detailed study excluded the formation of pure A type carbonate apatite. In turn, CO3- content in synthetic carbonate-substituted hydroxyapatite decreased. The usefulness of ATR-FTIR spectroscopic imaging studies in the evaluation of elastic and porous beta-glucan hydroxyapatite composites has been demonstrated. (C) 2016 Elsevier B.V. All rights reserved.

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