Szczegóły publikacji

Opis bibliograficzny

Microstructure characterization of advanced protective $Cr/CrN+a-C:H/a-C:H:Cr$ multilayer coatings on carbon fibre composite (CFC) / L. Major, M. Janusz, J. M. Lackner, M. KOT, B. Major // Journal of Microscopy ; ISSN 0022-2720. — 2016 — vol. 262 iss. 3, s. 191–202. — Bibliogr. s. 201–202, Summ. — Publikacja dostępna online od: 2016-01-20

Autorzy (5)

  • Major Łukasz
  • Janusz Maciej
  • Lackner Juergen Markus
  • AGHKot Marcin
  • Major Bogusław

Słowa kluczowe

multi-layer coatingsTEMwear mechanismsmicroanalysismicrostructuretransmission electron microscopy

Dane bibliometryczne

ID BaDAP98296
Data dodania do BaDAP2016-07-29
Tekst źródłowyURL
DOI10.1111/jmi.12364
Rok publikacji2016
Typ publikacjiprzegląd
Otwarty dostęptak
Czasopismo/seriaJournal of Microscopy

Abstract

Studies of advanced protective chromium-based coatings on the carbon fibre composite (CFC) were performed. Multidisciplinary examinations were carried out comprising: microstructure transmission electron microscopy (TEM, HREM) studies, micromechanical analysis and wear resistance. Coatings were prepared using a magnetron sputtering technique with application of high-purity chromium and carbon (graphite) targets deposited on the CFC substrate. Selection of the CFC for surface modification in respect to irregularities on the surface making the CFC surface more smooth was performed. Deposited coatings consisted of two parts. The inner part was responsible for the residual stress compensation and cracking initiation as well as resistance at elevated temperatures occurring namely during surgical tools sterilization process. The outer part was responsible for wear resistance properties and biocompatibility. Experimental studies revealed that irregularities on the substrate surface had a negative influence on the crystallites growth direction. Chromium implanted into the a-C:H structure reacted with carbon forming the cubic nanocrystal chromium carbides of the Cr23C6 type. The cracking was initiated at the coating/substrate interface and the energy of brittle cracking was reduced because of the plastic deformation at each Cr interlayer interface. The wear mechanism and cracking process was described in micro- and nanoscale by means of transmission electron microscope studies. Examined materials of coated CFC type would find applications in advanced surgical tools.

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