Szczegóły publikacji
Opis bibliograficzny
Characterization of microporous oxide layer synthesized on Ti-6Al-7Nb alloy by micro-arc oxidation / T. MOSKALEWICZ, A. KRUK, M. KOT, S. Kayali, A. CZYRSKA-FILEMONOWICZ // Archives of Civil and Mechanical Engineering / Polish Academy of Sciences. Wrocław Branch, Wrocław University of Technology ; ISSN 1644-9665. — 2014 — vol. 14 iss. 3, s. 370–375. — Bibliogr. s. 374–375, Abstr.
Autorzy (5)
Słowa kluczowe
Dane bibliometryczne
| ID BaDAP | 81801 |
|---|---|
| Data dodania do BaDAP | 2014-06-18 |
| Tekst źródłowy | URL |
| DOI | 10.1016/j.acme.2013.09.002 |
| Rok publikacji | 2014 |
| Typ publikacji | artykuł w czasopiśmie |
| Otwarty dostęp |  |
| Czasopismo/seria | Archives of Civil and Mechanical Engineering |
Abstract
In this work a microporous oxide layer was formed on two phase (alpha+beta) Ti-6Al-7Nb titanium alloy by the micro-arc oxidation process in an electrolyte containing (CH3COO)(2)CaH2O and Na3PO4. The thickness of the surface layer was in the range of 2.7 mu m-3.6 mu m. Microstructure of the surface layer and the substrate alloy was characterized with use of scanning- and transmission electron microscopy as well as by X-ray diffractometry. The microstructure of the surface layer consisted of TiO2 rutile and anatase nanocrystals as well as of amorphous regions containing mainly Ti, Ca and O atoms and a minority of P, Al and Nb ones. The surface layer was highly porous. The open pores, with diameter up to 6 mu m, were homogenously distributed in the specimen surface. Electron tomography was used to investigate the pores morphology and spatial distribution. It was found that open pores exhibited a complex geometry. The closed pores had nearly spherical shape. Adhesion of the surface layer to the titanium alloy substrate was investigated by means of the scratch-test. The value of critical load L-C2=14 N indicates a good layer adhesion to the underlying substrate. (C) 2013 Politechnika Wroclawska. Published by Elsevier Urban & Partner Sp. z o.o. All rights reserved.
