Szczegóły publikacji
Opis bibliograficzny
The 3D imaging and metrology of CMSX-4 superalloy microstructure using FIB-SEM tomography method / Adam KRUK, Beata DUBIEL, Aleksandra CZYRSKA-FILEMONOWICZ // Diffusion and Defect Data – Solid State Data. Part B, Solid State Phenomena ; ISSN 1012-0394. — 2013 — vol. 197, s. 89–94. — Bibliogr. s. 94, Abstr. — STERMAT : Stereology and image analysis in Materials science : 9thinternational conference : Zakopane, 3rd–6thSeptember 2012
Autorzy (3)
Słowa kluczowe
Dane bibliometryczne
| ID BaDAP | 72365 |
|---|---|
| Data dodania do BaDAP | 2013-03-14 |
| DOI | 10.4028/www.scientific.net/SSP.197.89 |
| Rok publikacji | 2013 |
| Typ publikacji | referat w czasopiśmie |
| Otwarty dostęp | |
| Czasopismo/seria | Diffusion and Defect Data. Solid State Data, Part B. Solid State Phenomena |
Abstract
STEM-EDX and FIB-SEM tomography studies have been carried out to visualize three-dimensional morphology of the gamma' precipitates in different zones of ex-service turbine blade made of CMSX-4 single crystal superalloy. The results allowed the three dimensional analysis of the changes in microstructure of blade as resulting of operating conditions. Tomographic reconstructions provided quantitative data about gamma and gamma' phase shape, size and volume fraction. It was shown that FIB-SEM tomography technique is suitable for 3D reconstruction of the objects of 100 urn in size or even smaller and thus enables the accurate quantitative microstructural analysis of this superalloy.