Szczegóły publikacji

Opis bibliograficzny

Applicability of the silver amalgam electrode in voltammetric determination of zinc and copper in gastric juice and gastric mucosa of rats / Włodzimierz Opoka, Bogusław BAŚ, Witold RECZYŃSKI, Małgorzata Płonka, Danuta Drozdowicz, Zbigniew Śliwowski, Tomasz Brzozowski // Acta Poloniae Pharmaceutica Drug Research ; ISSN 0001-6837. — 2011 — vol. 68 nr 4, s. 481–492. — Bibliogr. s. 491–492, Abstr.

Autorzy (7)

Słowa kluczowe

amalgam film electrodesatomic absorption spectrometrycopperzincstripping voltammetrygastric mucosagastric juice

Dane bibliometryczne

ID BaDAP60184
Data dodania do BaDAP2011-07-15
Tekst źródłowyURL
Rok publikacji2011
Typ publikacjiartykuł w czasopiśmie
Otwarty dostęptak
Creative Commons
Czasopismo/seriaActa Poloniae Pharmaceutica Drug Research

Abstract

The aim of the work was to compare two analytical methods of trace analysis in respect to their applicability in heavy metals determination in biological samples. Atomic absorption spectrometry (AAS) may be considered as the method of choice in such analyses due to its accuracy, precision and low detection limit. On the other hand, voltammetric methods seem to be as useful, but rarely applied. Having in mind that there is no universal analytical method, we have compared two AAS and voltammetric methods as the tools for Zn and Cu determination in the samples collected from rat gastric juice and gastric mucosa. Construction of the renewable silver amalgam film electrode (Hg(Ag)FE) for stripping voltammetry was described. Detailed optimization of measurements procedure and sample preparation for differential pulse anodic stripping voltammetry (DP ASV) and AAS were also performed and presented. The obtained results of quantitative analysis of the chosen parameters by means of both methods are discussed.

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