Szczegóły publikacji
Opis bibliograficzny
Dynamical simulation of on-axis transmission Kikuchi and spot diffraction patterns, based on accurate diffraction geometry calibration / Tianbi Zhang, Raynald Gauvin, Aimo WINKELMANN, T. Ben Britton // Journal of Microscopy ; ISSN 0022-2720 . — 2026 — vol. 303 iss. 2, s. 139–153. — Bibliogr. s. 152–153, Abstr. — Publikacja dostępna online od: 2026-05-19. — A. Winkelmann - dod. afiliacja: ST Development GmbH, Paderborn, Germany
Autorzy (4)
- Zhang Tianbi
- Gauvin Raynald
- AGHWinkelmann Aimo
- Britton T. Ben
Słowa kluczowe
Dane bibliometryczne
| ID BaDAP | 169601 |
|---|---|
| Data dodania do BaDAP | 2026-09-25 |
| Tekst źródłowy | URL |
| DOI | 10.1111/jmi.70119 |
| Rok publikacji | 2026 |
| Typ publikacji | artykuł w czasopiśmie |
| Otwarty dostęp |  |
| Creative Commons | |
| Czasopismo/seria | Journal of Microscopy |
Abstract
Transmission Kikuchi diffraction in the scanning electron microscope has gained popularity as a materials characterisation technique for its high throughput and nanometre-level spatial resolution. While conventional diffraction pattern analysis routines focus on Kikuchi bands on the diffraction patterns, the full physical picture of electron scattering and diffraction pattern formation is more complex. Analysis that accounts for additional diffraction features such as diffraction spots and excess-deficiency effects should provide more robust and accurate indexing, if they can be incorporated in pattern indexing or simulation routines. A more accurate understanding of their physics of formation and geometry is required to enable this change. In this work, we demonstrate geometric and full contrast dynamical simulation of on-axis transmission Kikuchi patterns, based on experimental patterns captured using a modular, direct electron detector-based set-up in the scanning electron microscope. First, a diffraction geometry calibration routine is proposed based on the electron channelling pattern of the direct electron detector. This allows us to accurately account for the position of diffraction spots in both geometric and dynamical simulations with good agreement with experimental patterns. Further, by introducing appropriate weight factors, simulation of incoherent diffuse intensity, and calculation of the energy spectra of diffracted electrons, simulated patterns can be obtained which accurately capture the many diffraction features on experimental patterns. Workflows and findings of this work can be used to improve pattern indexing routines, as well as the understanding of the physical processes in the formation of on-axis transmission Kikuchi patterns.
