Szczegóły publikacji
Opis bibliograficzny
A new era in ceramic archaeometry: a comprehensive multimodal methodological workflow / R. ABDELRAHMAN, J. Depciuch, P. GRZYWA, S. WROŃSKI, L. Alluhaibi, M. ŚRODA, A. Maximenko, M. Wojenka, J. TARASIUK, L. SAMEK // Acta Physica Polonica . A ; ISSN 0587-4246. — 2026 — vol. 149 no. 5, s. S198–S210. — Bibliogr. s. 209–210, Abstr. — Publikacja dostępna online od: 2026-05-26. — R. Abdelrahman - dod. afiliacja: Future University in Egypt, New Cairo, Egypt
Autorzy (10)
- AGHAbdelrahman Romisaa Gamal Mahmoud
- Depciuch Joanna
- AGHGrzywa Patryk
- AGHWroński Sebastian
- Alluhaibi Lulu
- AGHŚroda Marcin
- Maximenko Alexei A.
- Wojenka Michał
- AGHTarasiuk Jacek
- AGHSamek Lucyna
Słowa kluczowe
Dane bibliometryczne
| ID BaDAP | 167943 |
|---|---|
| Data dodania do BaDAP | 2026-05-28 |
| Tekst źródłowy | URL |
| DOI | 10.12693/APhysPolA.149.S198 |
| Rok publikacji | 2026 |
| Typ publikacji | artykuł w czasopiśmie |
| Otwarty dostęp |  |
| Creative Commons | |
| Czasopismo/seria | Acta Physica Polonica, A |
Abstract
This study establishes a comprehensive, sequential multimodal workflow for archaeometric analysis of medieval ceramics, integrating seven measurement techniques to characterize elemental, crystalline, amorphous, microstructural, structural, and chemical-state properties of the material, while preserving artefact integrity. Therefore, (i) X-ray fluorescence establishes baseline major (Si, Al, Fe, Ca, K, Na) and trace (Cr, Mn, Zr) profiles for paste discrimination; (ii) X-ray diffraction identifies kaliophilite/oligoclase phases (~ 800–900°C firing); (iii) Fourier transform infrared resolves amorphous networks (Si–O–Si 950–1100 cm-1); (iv) Raman spectroscopy detects microscale oxide impurities (anatase TiO2 lattice modes at 110–160 cm-1, ZrO2, Al2O3 corundum M–O stretching modes at 440–465 cm-1) and lattice defects, revealing heavy mineral tempers (rutile sands) and refractory phases undetectable by bulk diffraction analysis or the broad spectral envelopes of infrared spectroscopy; (v) scanning electron microscope with energy dispersive spectroscopy quantifies temper distributions; (vi) X-ray computed tomography reveals 3D void networks, and (vii) X-ray absorption near-edge structure constrains speciation of Fe2+/Fe3+, Ca carbonate–silicates, and K-feldspars. This standardized framework enables precise reconstruction of provenance, fluxing strategies, pyrotechnology, and post-firing alterations, beyond the limitations of single- and dual-technique approaches, providing a reproducible protocol for heritage science.
