Szczegóły publikacji

Opis bibliograficzny

Mechanical properties and biocompatibility of multilayer systems based on amorphous SiN:H/SiCN:H layers on Ti6Al7Nb titanium alloy / Łukasz Kaczmarek, Agnieszka Kyzioł, Daniel Kottfer, Witold Szymański, Kamil KLESZCZ, Karol KYZIOŁ // Applied Surface Science ; ISSN  0169-4332 . — Tytuł poprz.: Applications of Surface Science. — 2024 — vol. 675 art. no. 160947, s. 1–12. — Bibliogr. s. 11–12, Abstr. — Publikacja dostępna online od: 2024-08-11

Autorzy (6)

Słowa kluczowe

Ti6Al7Nb alloyamorphous multi layersMW CVD plasma techniqueSiCN:Hmechanical propertiesbiocompatibility

Dane bibliometryczne

ID BaDAP155087
Data dodania do BaDAP2024-09-30
Tekst źródłowyURL
DOI10.1016/j.apsusc.2024.160947
Rok publikacji2024
Typ publikacjiartykuł w czasopiśmie
Otwarty dostęptak
Creative Commons
Czasopismo/seriaApplied Surface Science

Abstract

Surfaces of metallic implants that replace diseased joints are bound to degrade over time under constant mechanical wear and corrosion, caused by the presence of biological fluids. Production of wear particles and toxic metal ions that follows can undermine both implant stability and patient's health. To counteract this process multiple surface modifications have been proposed in scientific literature, ranging from simple nitriding to protective layers (e.g.: DLC, CN:H) and multilayer systems. This work presents a combined approach to outlined issue, using multi-staged plasma deposition with SiCN:H layer as a key component, realized using the MW CVD (Microwave Chemical Vapour Deposition) system. The study covers chemical characterization by EDS and FTIR analysis and measurements of relevant functional parameters, such as hardness, Young's modulus, coefficient of friction, specific wear rate and wettability. Additionally, biocompatibility of modified surfaces are tested on MG-63 cells using Alamar Blue assay, flow cytometry and alkaline phosphatase (ALP) assay. Chemical and microscopic studies revealed amorphous cauliflower-like microstructures that have proven to be hydrogenated SiCN/SiN structures. The obtained layers are turned out to be biocompatible (>70 % of cell survival rate), additionally layers based on amorphous SiCN:H boost ALP activity due to combination of their chemistry and mechanical properties.

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