Szczegóły publikacji
Opis bibliograficzny
Synthesis of conical Co–Fe alloys structures obtained with crystal modifier in superimposed magnetic field / Katarzyna SKIBIŃSKA, Dawid KUTYŁA, Karolina KOŁCZYK-SIEDLECKA, Mateusz M. MARZEC, Piotr ŻABIŃSKI, Remigiusz KOWALIK // Archives of Civil and Mechanical Engineering / Polish Academy of Sciences. Wrocław Branch, Wrocław University of Technology ; ISSN 1644-9665. — 2021 — vol. 21 iss. 4 art. no. 165, s. 1–11. — Bibliogr. s. 10–11, Abstr. — Publikacja dostępna online od: 2021-10-11
Autorzy (6)
Słowa kluczowe
Dane bibliometryczne
ID BaDAP | 137062 |
---|---|
Data dodania do BaDAP | 2021-10-22 |
Tekst źródłowy | URL |
DOI | 10.1007/s43452-021-00315-2 |
Rok publikacji | 2021 |
Typ publikacji | artykuł w czasopiśmie |
Otwarty dostęp | |
Creative Commons | |
Czasopismo/seria | Archives of Civil and Mechanical Engineering |
Abstract
The addition of crystal modifier to electrolyte used during electrodeposition of metals and alloys allows obtaining conical structures without using any template. This method is fast and ensures covering large areas during one single electrodeposition process. In this work, Co–Fe cones were obtained by one-step method with ammonium chloride as a crystal modifier. The influence of electrodeposition parameters and electrolyte compositions were investigated. Electrodeposition conditions (duration, electrolyte temperature, and addition of NH4Cl), which allow obtaining the most uniform conical structures, were applied during sample fabrication in the magnetic field. The influence of its value and direction on the quality and compositions of obtained alloys was investigated using Scanning Electron Microscope (SEM) photos. To check if there is any change in the sample crystal system, the X-Ray Diffraction (XRD) analysis was performed. To confirm the synthesis of Co–Fe cones, they were analyzed using the X-ray photoelectron Spectroscopy (XPS) method.