Szczegóły publikacji

Opis bibliograficzny

Application of analytical electron microscopy and FIB-SEM tomographic technique for phase analysis in as-cast Allvac 718Plus superalloy / Adam KRUK, Grzegorz CEMPURA // International Journal of Materials Research ; ISSN 1862-5282. — Tytuł poprz.: Zeitschrift für Metallkunde. — 2019 — vol. 110 iss. 1, s. 3–10. — Bibliogr. s. 9–10. — Publikacja dostępna online od: 2018-07-16. — XVI international conference on Electron microscopy : Jachranka, Poland, September 10th-13th 2017

Autorzy (2)

Słowa kluczowe

ATI Allvac 718PlusFIB SEM tomographyLaves phaseSTEM-HAADFSEM-EDS

Dane bibliometryczne

ID BaDAP119500
Data dodania do BaDAP2019-02-07
Tekst źródłowyURL
DOI10.3139/146.111678
Rok publikacji2019
Typ publikacjireferat w czasopiśmie
Otwarty dostęptak
Creative Commons
Czasopismo/seriaInternational Journal of Materials Research

Abstract

The superalloys are usually used as structural material in jet engines due to their high-temperature stability and good endurance. Many components found in the hot-part of jet engines are of complex shape, therefore casting is utilized for to their production. One of the problems associated with the casting process of highly alloyed alloys, such as superalloys, is partitioning of alloying elements upon solidification. This segregation might lead to the formation of low melting temperature eutectics. Their presence in the material microstructure will have a negative effect on the weldability. Negative impact on weldability is one of the reasons why secondary phases should be avoided as microstructural elements in the welded materials. To eliminate such hazardous phases, the material should be subjected to a heat treatment with the aim of homogenizing the microstructure and chemical composition, which should enhance the weldability. The aim of this work was the application of analytical electron microscopy in combination with energy dispersive X-ray spectroscopy as well as tomographic techniques for qualitative and quantitative characterization of structural elements in as-cast Allvac 718Plus Ni-based superalloy subjected to later heat treatment. Alloy 718Plus is a newly developed superalloy in which the secondary Laves phase forms as a low-melting eutectic upon casting. The development of innovative materials for aeronautics and clean energy systems requires the use of modern research methods for structure characterization on the level from micro- to the nanoscale. The performed analysis, allowed identification of phases (Laves and η) occurring in interdendritic regions of as-cast Allvac 718Plus superalloy and analyzing their microstructure down to the atomic scale, which revealed their complex nature. The experiments and investigation show that advanced microscopic techniques and test methods in conjunction with tomographic techniques enable complementary information about solidified structures of the alloy to be obtained that can be useful for the understanding process of casting and welding of the Allvac 718Plus.

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artykuł
#98636Data dodania: 28.7.2016
STEM-EDX and FIB-SEM tomography of Allvac 718Plus superalloy / A. KRUK, G. CEMPURA, S. LECH, A. CZYRSKA-FILEMONOWICZ // Archives of Metallurgy and Materials / Polish Academy of Sciences. Committee of Metallurgy. Institute of Metallurgy and Materials Science ; ISSN 1733-3490. — 2016 — vol. 61 no. 2A, s. 535–541. — Bibliogr. s. 541
fragment książki
#114776Data dodania: 2.7.2018
Application of analytical electron microscopy and tomographic techniques for metrology and 3D imaging of microstructural elements in $Allvac^®$ 718Plus™ / A. KRUK, G. CEMPURA, S. LECH, A. M. Wusatowska-Sarnek, A. CZYRSKA-FILEMONOWICZ // W: Proceedings of the 9th international symposium on superalloy 718 & derivatives: energy, aerospace, and industrial applications / ed. Eric Ott, [et al.]. — Cham : Springer International Publishing AG, 2018. — (The Minerals, Metals & Materials Series ; ISSN 2367-1181). — ISBN: 978-3-319-89479-9; e-ISBN: 978-3-319-89480-5. — S. 1035–1050. — Bibliogr. s. 1049–1050, Abstr. — Toż. na pendrive