Szczegóły publikacji

Opis bibliograficzny

The 3D imaging and metrology of microstructural elements in innovative materials for clean energy systems and aeronautics / Adam KRUK, Aleksandra CZYRSKA-FILEMONOWICZ // Materials Science Forum ; ISSN 0255-5476. — Tytuł poprz.: Diffusion and Defect Monograph Series. — 2017 — vol. 879, s. 1019–1024. — Bibliogr. s. 1024, Abstr. — Publikacja dostępna online od: 2016-11-15. — THERMEC'2016 : 9th international conference on processing and manufacturing of advanced materials : May 28 – 3 June 2016, Graz, Austria

Autorzy (2)

Słowa kluczowe

FIB SEM tomographySTEM-EDX tomographyAllvac 718Plus

Dane bibliometryczne

ID BaDAP102401
Data dodania do BaDAP2016-12-21
Tekst źródłowyURL
DOI10.4028/www.scientific.net/MSF.879.1019
Rok publikacji2017
Typ publikacjireferat w czasopiśmie
Otwarty dostęptak
Czasopismo/seriaMaterials Science Forum

Abstract

The aim of this study was presentation the results of new tomographic techniques application to characterize structural elements in nickel-based superalloys for disc and blades using in aircraft engines and gas turbines in energy systems. Visualization of phases presented in as-service high chromium creep resistant steel for modern power plant applications was also performed using STEM-EDX and FIB-SEM electron tomography. Electron tomography (STEM-EDX) and FIB-SEM tomography were used for 3D imaging and metrology of the precipitates. Transmission electron microscopy and TEM-EDX spectroscopy were used to reveal details of the superalloys and steel microstructures and phases’ chemical compositions. The study showed that electron tomography techniques permit to obtain complementary information about microstructural features (precipitates size, shape and their 3D distribution) in the reconstructed volume with comparison to conventional particle analysis methods, e.g. quantitative TEM and SEM metallography.

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